Teledyne Leeman Labs Blog

ICP-OES instruments used to analyze mining waste from abandoned copper mines

Posted by Betsey Seibel on Oct 20, 2014 11:02:15 AM

Less than 40 years ago in 1978, the Communist dictator of Romania ordered the 400 families living in the small village of Geamana to leave their homes so that the country could build a copper mine. Unfortunately, the people did not have much choice as the village was to become an artificial lake for the toxic waste from the Rosia Poieni, one of Europe’s largest copper mines. The water that covers Geamana is laced with cyanide and other chemicals, making the area uninhabitable. Recently, the website Roadtrippers published several pictures from the abandoned village.

Unfortunately, the fate of Geamana is not uncommon. In the United States, the area around Treece, Kansas and Picher, Oklahoma was ranked in 1981 by the Environmental Protection Agency as the most contaminated in the country. The contamination was the result of extensive lead and zinc mining. In the 1920s, the area was the number one producer of the elements in the United States, supplying the metals for ammunition during the World Wars. While the metals were extracted, the waste was piled up around the town into mounds of contaminated gravel that still litter the landscape. A New York Times article from May 2012, describe the conditions:

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Tags: ICP-OES, Inductively Coupled Plasma, Interest Stories

Soil Lead Contamination Leads to Massive Cleanup

Posted by Betsey Seibel on Oct 8, 2014 2:03:01 PM

More than 144 homes in a two-square mile southeast of Los Angeles County are the focus of lead contamination test after the California Department of Toxic Substances Control detected high levels of lead in soil near a temporarily closed battery recycling plant. In the fall of 2013, elevated levels of lead at 39 homes and a preschool near the plant were blamed on air pollution from the plant and prompted local officials to issue health warnings and push for additional testing. State regulators expanded the lead soil testing to include more than 144 homes in Vernon, California.

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Tags: ICP-OES, Lead Contamination

Mercury Contamination Causing Major Health Problems in Birds - Need for Mercury analysis in water and food

Posted by Betsey Seibel on Oct 1, 2014 2:08:12 PM

Recently more 750 scientists from around the world gathered at the Animal Behavior Society meeting at Princeton University. They gathered to discuss… you guessed it… animals; all kinds of animals, from fish to birds. Among the topics of discussions was the impact of liquid metal mercury, even small doses, on the animal kingdom, particularly in birds. In humans, large doses of mercury can cause lethargy and depression, while smaller amounts can lead to dementia. In animals that are much smaller, the impact can be even more significant.

Researchers at the College of William and Mary conducted an experiment where they exposed zebra finches to mercury levels consistent with a contaminated environment. Rather than lethargy or depression, the finches exhibited symptoms more on the side of dementia. The birds were “bolder and hyperactive,” and “spent less time feeding” compared with birds that had not been exposed to the metal. Because of this behavior, the finches could be at risk of increased predation. Unfortunately, they discovered some other disturbing trends.

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Tags: Hg analysis, mercury

Do Cavities Contribute to Mercury Pollution?

Posted by Betsey Seibel on Sep 29, 2014 7:46:00 PM

Where does roughly half of all mercury that enters public water treatment systems come from?

If you answered dental offices, you would be correct.

According the U.S. Environment Protection Agency 120,000 dental offices use or dispose of amalgam fillings, which contain a mixture of mercury and other metals used in dental fillings.  Most of these offices are attached to public sewer systems. The amalgam waste is flushed at the point-of-care down chair-side drains. When the amalgam is discharged into the sewer systems, it can be transformed into methylmercury, which is a highly toxic neurotoxin that impairs brain and nervous system development and function. Methylmercury can build up in fish, shellfish and fish-eating animals, which can be harmful to humans who consume the fish.

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Tags: Hg analysis, mercury

Frequently Asked Questions about EPA Method 245.7

Posted by Betsey Seibel on Sep 19, 2014 4:17:25 PM

We thought it might be helpful for those of you with questions regarding EPA Method 245.7 to create a blog post addressing some of these questions.  If you have any questions regarding EPA 245.7 that we haven't addressed here, please let us know and we will do our best to provide you with the answer.

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Tags: CVAF, Hg analysis, mercury analysis

Humans are Major Cause of Mercury Levels in Ocean Surface Waters

Posted by Betsey Seibel on Aug 19, 2014 4:18:00 PM

A new paper by researchers from the Woods Hole Oceanographic Institution (WHOI), Wright State University, Observatoire Midi-Pyréneés in France, and the Royal Netherlands Institute for Sea Research found that the ocean contains about “60,000 to 80,000 tons of pollution mercury. In addition, they found that ocean waters shallower than about 100 m (300 feet) have tripled in mercury concentration since the Industrial Revolution and that the ocean as a whole has shown an increase of roughly 10 percent over pre-industrial mercury levels.”[i] The paper, which appears in a recent addition of the journal of Nature “provides the first direct calculation of mercury in the global ocean from pollution based on data from 12 sampling cruises over the past 8 years,” and “a look at the global distribution of mercury in the marine environment.”


While mercury is a naturally occurring element, it is also a by-product of human mining and manufacturing operations, from burning coal to making cement. The researchers set out to better understand how much of the mercury in the ocean is a result of human activity or how much is from natural sources. The group looked at data about oceanic levels of phosphate, and by “determining the ratio of phosphate to mercury in water deeper than 1,000 meters (3,300 feet) that has not been in contact with Earth's atmosphere since the Industrial Revolution, the group was able to estimate mercury in the ocean that originated from natural sources such as the breakdown, or ‘weathering,’ of rocks on land.”

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Tags: mercury analysis

Thoughts to Communities Impacted by Mount Polley Mine Breach

Posted by Betsey Seibel on Aug 14, 2014 11:57:00 AM

One week after a tailings pond dam burst at Mount Polley Mine near the cities of Williams Lake and Quesnel, British Columbia, environmental experts are saying it could be one of the worst tailings pond breaches in the world. Early estimates suggest that more than 2.64 billion gallons of mining waste and 4.5 million cubic meters of ground-up rock were released into Polley Lake, Quesnel Lake, Hazeltine Creek and Cariboo Creek. According to the mine’s owners 2013 mine report, substances that are disposed of on-site into the pond include arsenic, copper, lead, manganese, mercury, phosphorus, and selenium; among several other metals. Days following the breach, hundreds of local residents were banned from using the water for drinking or bathing, campgrounds were evacuated, fishing was banned and an emergency was declared.

As a company, we were saddened to read about the breach and by its initial and impending impact. Our first thoughts are with the people and communities in British Columbia who are suffering through this unfortunate situation. This type of disaster can have a devastating impact on the local ecosystem, and its clear that a massive waste removal project will be required in the future. Many are comparing this to a tailings pond breach in Tennessee in 2008, where cleanup was slow and estimated at $600-800 million. Monitoring the rise in toxins absorbed by fish and wildlife has started, and officials are conducting regular water quality tests of area resources to better understand the aftermaths. On a positive note, an early round of tests completed last week found that water “samples indicate that none of the chemical and physical parameter concentrations exceeded B.C. or Health Canada drinking water guidelines.” Unfortunately, “All five testing sites also had zinc levels above chronic, or long-term, exposure limits for aquatic life.”

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Tags: Mining, Interest Stories

Tungsten Carbide Production and Quantification of Purity using a DC Arc Spectrometer

Posted by Jason Davis on Aug 4, 2014 12:55:31 PM

Tungsten Carbide (also called cemented carbide or simply carbide) is a metal composite created from tungsten carbide and a binder metal (usually cobalt or nickel) in powder form that is compacted and sintered in a furnace. Tungsten Carbide is used for tools, abrasives, jewelry, industrial drills, and armor-piercing ammunition due to its exceptional hardness (8.5-9.0, surpassed only by diamonds). Because the tungsten carbide particles are captured in a binder during the sintering process, the result is referred to as “cemented”.

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Tags: Teledyne Leeman Labs, Prodigy DC Arc Spectrometer, High-Purity WC

Copper Ore to High-Purity Copper, and the Quantification of Purity

Posted by Jason Davis on Jul 22, 2014 8:54:14 AM

Modern copper ores contain less than 0.6% copper, and less than 2% total volume of economic ore minerals (including copper). A majority of the ore is comprised of unwanted rock and gangue minerals (typically silicate minerals or oxide minerals). Separation of ore minerals from gangue minerals entails complicated and labor intensive processes.

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Tags: Teledyne Leeman Labs, Prodigy DC Arc, High-Purity Copper, Determination of Trace Elements, Sulphur in High-Purity Copper, Grade 1 Cathode Copper, Cu

Water Quality Considerations for Mercury Analysis (EN17852 /USEPA 245.7)

Posted by Betsey Seibel on Oct 22, 2013 9:51:00 AM

When it comes to mercury analysis using Atomic Fluorescence Spectrometry there are two main methods to use - USEPA Method 245.7 and The European Norm EN17852 Water Quality - Determination of Mercury - Method using atomic fluorescence spectrometry (ISO 17852:2006).  

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Tags: mercury analysis, EN17852, USEPA 245.7